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molbloc-S Sonic Nozzle Calibration Device

molbloc-S sonic nozzle calibration device
molbloc-S Sonic Nozzle Flow Element
molbloc-S sonic nozzle calibration device
molbloc-S Sonic Nozzle Flow Element
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  • Highlights
  • Description
  • Specifications
  • Models and Accessories
  • Knowledge and Information

Sonic nozzle based molblocs for gas flow up to 5,000 slm

molbloc-S® Sonic Nozzle Flow Element is a high precision transfer standard intended for calibrating other transfer standards or process flow meters and controllers. This sonic nozzle calibration device is used with molbox1+ or molbox RFM™ terminals to extend the range of molbloc/molbox™ calibration systems and deliver superior accuracy at medium and high flows. Existing molbox1 terminals with version 4.0 embedded software or later and all molbox1+ terminals can be used with molbloc-S.

Features at a glance

  • Covers ranges up to 5,000 slm in N2 and air
  • Useable with molbox1+, or existing molbox1 and molbox RFM mass flow terminals and COMPASS software
  • Proven critical flow venturi (sonic) nozzle operating principle supported by gravimetric calibration
  • Minimal sensitivity to contamination
  • Measurement uncertainty:
    to ±0.125% of reading with molbox1+
    ± 0.2 % of reading with molbox1
    ± 0.5 % of reading with molbox RFM
  • Air, N2, Ar, He and other calibrations available, humid air density compensation supports use with ambient air
  • Excellent rangeability (10:1 turndown), with molbox1+S, or other molbox models with vacuum.
  • Redundant absolute upstream pressure measurement using both molbox absolute pressure transducers reduces uncertainty and increases reliability
  • Integral gas temperature conditioning and measurement
  • Continuous, real-time reading, as with traditional molbloc-L laminar element
  • Can be fully automated

molbloc-S ranges

The mass flow rate through molbloc-S Sonic Nozzle is directly proportional to the upstream absolute pressure and independent of the downstream or differential pressure. molbloc-S flow ranges are defined by the molbloc's Pressure to Flow Conversion Ratio, KF. KF is expressed in units of sccm/kPa and defines the relationship between mass flow and the absolute upstream pressure delivered to the molbloc-S. molbloc-S calibrations are performed over flow ranges corresponding to either 20 to 200 kPa (3 to 30 psia), 50 to 500 kPa (7 to 70 psia) or 200 kPa to 2 MPa (30 to 300 psia) upstream pressure.

For flow measurements to be valid, the flow at the throat of the molbloc-S venturi nozzle must be critical, i.e. the gas speed is equal to the local speed of sound. Critical flow is achieved when a sufficiently low back pressure ratio, or BPR (molbloc-S downstream absolute pressure divided by upstream absolute pressure) is maintained. The upper limit of acceptable molbloc-S BPR values for critical flow varies between about 0.5 and 0.9 depending on the Reynolds number of the flow.

Since the mass flow through molbloc-S is proportional to the upstream absolute pressure, the flow range for this sonic nozzle calibration device in an application may be limited by the BPR limit. To maximize the range of a molbloc-S element, a vacuum pump can be connected downstream to reduce the downstream pressure while flowing. When the downstream pressure is kept sufficiently low, the upstream pressure, and thus the mass flow rate, can be adjusted all the way down to the minimum value for the molbloc's calibration type without being limited by the BPR. If molbloc-S will be used with atmospheric pressure downstream (no vacuum pump), then the molbloc can only be used over a range of upstream pressures starting at the maximum pressure for its calibration type down to a minimum pressure value at which the BPR becomes equal to the BPR limit at the current Reynolds number. molbox1 terminals include features to measure BPR, automatically alert the operator when the BPR is too high and prevent measurements when flow is not critical.

molbloc/molbox specifications - General

  molbox1+ molbox RFM
All specifications same molbox1 unless specified otherwise.
Normal Operating Temperature Range: 15 to 35 °C  
Storage Temperature Range: -25 to 35 °C  
Normal Operating Pressure Range: 20 to 200 kPa absolute (3 to 30 psia) or 50 to 500 kPa absolute (7 to 70 psia) upstream, or 200 to 2000 kPa (30 to 300 psia) with molbox1+S only.  
Overall Flow Range: <1 to 5 000 slm  
Inlet Connection:
1E1-S thru 1E2-S
2E2-S thru 2E3-S
5E3-S and 1E4-S
1/4 in. VCR™
1/2 in. VCR™
1 in. VCR™ or 1 in. NPT
 
Outlet Connection:
5E1-S thru 2E3-S
5E3-S, 1E4-S
16 mm (3/4 in.) ISO-KF style vacuum flange
40 mm (1 1/2 in.) ISO-KF style vacuum flange
 
Gases Supported: Nitrogen (N2), Dry Air, Humid Air, Argon (Ar), Carbon Monoxide (CO), Helium (He), Oxygen (O2), Carbon Dioxide (CO2), Carbon Tetrafluoride (CF4), Ethane (C2H6), Ethylene (C2H4), Fluoroform (CHF3), Hexafluoroethane (C2F6), Hydrogen (H2), Methane (CH4), Nitrous Oxide (N2O), Propane (C3H8), Sulfur Hexafluoride (SF6), Butane (C4H10), Octafluorocyclobutane (C4F8), Xenon (Xe)  

Flow Measurement

Range: Dependent upon molbloc size and pressure calibration range (see molbloc-S Ranges table)  
Required Back Pressure Ratio: 0.4 to 0.9 depending on Reynolds number  
Calibration Gases: Standard: Dry air

Optional: N2 (to replace standard air calibration or in addition), Ar, H2, He, N2O. Consult factory regarding availability of availability of these gases for specific ranges, or for other gases.

*Dry air calibration is required for humid air operation

 
molbloc-S Pressure Calibration Ranges: Low Pressure (LP):
20 to 200 kPa absolute (3 to 30 psia) upstream

Standard Pressure (SP):
50 to 500 kPa absolute (7 to 70 psia) upstream

High Pressure (HP):
200 to 2 MPa absolute (30 to 300 psia) upstream

* HP calibration usable with molbox1+S terminal only
* Flow measurement specifications valid from 10% to 100% of molbloc full scale

 
Resolution: ± 0.0015 % of FS ± 0.01 % of reading
Precision: ± 0.06 % of reading ± 0.30 % of reading
Predicted Stability (One Year): ± 0.05 % of reading ± 0.2 % of reading
Measurement Uncertainty ± 0.2 % of reading
Premium calibration: ± 0.125 % of reading
± 0.5 % of reading from 50 to 500 kPa
Model Name Description
1E1-S

KF [sccm/kPa]: 10

Each molbloc-S is delivered complete with:

  • molbloc-S flow element
  • Shipping and storage case
  • Soft, reusable VCR O-rings for molbloc upstream connection; ISO-KF style centering ring, clamp and overpressure ring for molbloc downstream connection; mounting instructions
  • Standard uncertainty calibration at standard pressure (SP) with air and accredited calibration report.

Premium uncertainty, HP or LP pressure calibrations and other calibration gases available - consult agent or factory.

2E1-S

KF [sccm/kPa]: 20

Each molbloc-S is delivered complete with:

  • molbloc-S flow element
  • Shipping and storage case
  • Soft, reusable VCR O-rings for molbloc upstream connection; ISO-KF style centering ring, clamp and overpressure ring for molbloc downstream connection; mounting instructions
  • Standard uncertainty calibration at standard pressure (SP) with air and accredited calibration report.

Premium uncertainty, HP or LP pressure calibrations and other calibration gases available - consult agent or factory.

5E1-S

KF [sccm/kPa]: 50

Each molbloc-S is delivered complete with:

  • molbloc-S flow element
  • Shipping and storage case
  • Soft, reusable VCR O-rings for molbloc upstream connection; ISO-KF style centering ring, clamp and overpressure ring for molbloc downstream connection; mounting instructions
  • Standard uncertainty calibration at standard pressure (SP) with air and accredited calibration report.

Premium uncertainty, HP or LP pressure calibrations and other calibration gases available - consult agent or factory.

1E2-S

KF [sccm/kPa]: 100

Each molbloc-S is delivered complete with:

  • molbloc-S flow element
  • Shipping and storage case
  • Soft, reusable VCR O-rings for molbloc upstream connection; ISO-KF style centering ring, clamp and overpressure ring for molbloc downstream connection; mounting instructions
  • Standard uncertainty calibration at standard pressure (SP) with air and accredited calibration report.

Premium uncertainty, HP or LP pressure calibrations and other calibration gases available - consult agent or factory.

2E2-S

KF [sccm/kPa]: 200

Each molbloc-S is delivered complete with:

  • molbloc-S flow element
  • Shipping and storage case
  • Soft, reusable VCR O-rings for molbloc upstream connection; ISO-KF style centering ring, clamp and overpressure ring for molbloc downstream connection; mounting instructions
  • Standard uncertainty calibration at standard pressure (SP) with air and accredited calibration report.

Premium uncertainty, HP or LP pressure calibrations and other calibration gases available - consult agent or factory.

5E2-S

KF [sccm/kPa]: 500

Each molbloc-S is delivered complete with:

  • molbloc-S flow element
  • Shipping and storage case
  • Soft, reusable VCR O-rings for molbloc upstream connection; ISO-KF style centering ring, clamp and overpressure ring for molbloc downstream connection; mounting instructions
  • Standard uncertainty calibration at standard pressure (SP) with air and accredited calibration report.

Premium uncertainty, HP or LP pressure calibrations and other calibration gases available - consult agent or factory.

1E3-S

KF [sccm/kPa]: 1000

Each molbloc-S is delivered complete with:

  • molbloc-S flow element
  • Shipping and storage case
  • Soft, reusable VCR O-rings for molbloc upstream connection; ISO-KF style centering ring, clamp and overpressure ring for molbloc downstream connection; mounting instructions
  • Standard uncertainty calibration at standard pressure (SP) with air and accredited calibration report.

Premium uncertainty, HP or LP pressure calibrations and other calibration gases available - consult agent or factory.

2E3-S

KF [sccm/kPa]: 2000

Each molbloc-S is delivered complete with:

  • molbloc-S flow element
  • Shipping and storage case
  • Soft, reusable VCR O-rings for molbloc upstream connection; ISO-KF style centering ring, clamp and overpressure ring for molbloc downstream connection; mounting instructions
  • Standard uncertainty calibration at standard pressure (SP) with air and accredited calibration report.

Premium uncertainty, HP or LP pressure calibrations and other calibration gases available - consult agent or factory.

5E3-S

KF [sccm/kPa]: 5000

Each molbloc-S is delivered complete with:

  • molbloc-S flow element
  • Shipping and storage case
  • Soft, reusable VCR O-rings for molbloc upstream connection; ISO-KF style centering ring, clamp and overpressure ring for molbloc downstream connection; mounting instructions
  • Standard uncertainty calibration at standard pressure (SP) with air and accredited calibration report.

Premium uncertainty, HP or LP pressure calibrations and other calibration gases available - consult agent or factory.

1E4-S

KF [sccm/kPa]: 10,000

Each molbloc-S is delivered complete with:

  • molbloc-S flow element
  • Shipping and storage case
  • Soft, reusable VCR O-rings for molbloc upstream connection; ISO-KF style centering ring, clamp and overpressure ring for molbloc downstream connection; mounting instructions
  • Standard uncertainty calibration at standard pressure (SP) with air and accredited calibration report.

Premium uncertainty, HP or LP pressure calibrations and other calibration gases available - consult agent or factory.

molbloc-S Calibration Options

Low Pressure 20 to 200 kPa (3 to 30 psia)
upstream of the molbloc (specify premium or standard)

Standard Pressure 50 to 600 kPa (7 to 87 psia)
upstream of the molbloc (specify premium or standard)

High Pressure 200 to 2000 kPa (30 to 300 psia)
upstream of the molbloc (specify premium or standard)

Accessories common to all models:

Accessory Description
Priority Gold Instrument CarePlan

Fluke Calibration Priority Gold Instrument CarePlans are available for most calibration products. Please contact your local Fluke Calibration sales representative for details or to request a quote. You may also call the Customer Care Center at 877-355-3225 or send email to careplans@flukecal.com.

Product Manuals
application/pdf icon FTS Adaptor Kit for molbloc-S™ Installation and Operation Instructions (193.87 KB)
application/pdf icon Installation and Use of Low-Flow Vacuum Pump Kit for molbloc-S® Instruction Sheet (648.49 KB)
application/pdf icon Installation and Use of Medium-Flow Vacuum Pump Kit for molbloc-S® Installation Instructions (278.16 KB)
application/pdf icon Installation and Use of Vacuum Pump Downstream Interconnect Kit for molbloc-S® (215.22 KB)
application/pdf icon Installation of 1/4 in. and 1/2 in. molbloc-S® Inlet Flange Conversion Kits Instruction Sheet (176.92 KB)
application/pdf icon molbox1+™/molbox1+S molbloc® Terminal Operation and Maintenance Manual (1.66 MB)
application/pdf icon molbox1+™/molbox1+S molbloc® Terminal Operation and Maintenance Manual Supplement (67.75 KB)
application/pdf icon Operation of Adjustable DUT Stand for molbloc-S® Instruction Sheet (172.2 KB)
application/pdf icon PK-mol-4VCR-1/4SWG Adaptor Kit Installation Instructions (143.99 KB)
application/pdf icon PK-mol-KF Adaptor Kits for molbloc-S® Instruction Sheet (174.45 KB)
application/pdf icon Recommendations for molbloc-S® Downstream Tee Assembly Instruction Sheet (182.52 KB)
application/pdf icon Recommendations for molbloc-S® Installation Instruction Sheet (198.92 KB)
application/pdf icon Recommendations for molbloc™ Installation Instruction Sheet (186.92 KB)
Application Notes
application/pdf icon Four Steps to More Effective Gas Flow Calibration (1.33 MB)
application/pdf icon Quatre étapes pour un étalonnage plus efficace des débits de gaz (2.07 MB)
application/pdf icon Vier Schritte für eine effektivere Massendurchflusskalibrierung (2.08 MB)
application/pdf icon Hardware Setup and Application Notes for Calibrating FTS Device with molbloc/molbox™ (102.49 KB)
application/pdf icon Mass flow versus volume flow in gas flow calibration (769.59 KB)
application/pdf icon Uncertainty Analysis for Flow Measured by molbloc-L and molbloc-S Mass Flow Transfer Standards (224.38 KB)
application/pdf icon Principles of Metrology (400.44 KB)
Data Sheets
application/pdf icon molbloc-S ranges data sheet (172.57 KB)
application/pdf icon molbloc-S Sonic Nozzle Based molblocs for Gas Flow up to 5000 slm Technical Data (1.73 MB)
application/pdf icon molstic-S ™ Mounting System for molbloc-S ® Data Sheet (1.84 MB)
Video
molbox/molbloc Mass Flow Calibration Solution Demo Video
molbox: Gas Flow Calibration System
On-Demand Webinars
How to calibrate rotameters and other density-dependent flow meters
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